Effect of helium on irradiation creep behavior of B-doped F82H irradiated in HFIR

Ando, Masami; Nozawa, Takashi; Hirose, Takanori; Tanigawa, Hiroyasu; Wakai, Eiichi; Stoller, R. E.*; Myers, J.*

Fusion Science and Technology, 68(3), p.648 - 651, 2015/10

https://doi.org/10.13182/FST14-963

Pressurized tubes of F82H and B-doped F82H irradiated at 573 and 673 K up to 6dpa have been measured by a laser profilometer. The irradiation creep strain in F82H irradiated at 573 and 673 K was almost linearly dependent on the effective stress level for stresses below 260 MPa and 170 MPa, respectively. The creep strain of BN-F82H was similar to that of F82H IEA at each effective stress level except 294 MPa at 573 K irradiation. For 673 K irradiation, the creep strain of some BN-F82H tubes was larger than that of F82H tubes. It is suggested that a swelling caused in each BN-F82H because small helium babbles might be produced by a reaction of B(n, ) Li.

Effects of irradiation on mechanical properties of HIP-bonded reduced-activation ferritic/martensitic steel F82H first wall

Furuya, Kazuyuki; Wakai, Eiichi; Miyamoto, Kenji*; Akiba, Masato; Sugimoto, Masayoshi

Journal of Nuclear Materials, 367-370(1), p.494 - 499, 2007/08

https://doi.org/10.1016/j.jnucmat.2007.03.011

A partial mock-up of a breeding blanket structure made of F82H steel has been successfully fabricated. In this study, microstructural observation and EDX analysis of the HIP interfaces were performed, and effects of irradiation on mechanical properties of the HIP-bonded region were also examined. Neutron irradiation was performed up to about 2 dpa at about 523 K. After the irradiation, tensile test was performed at temperatures of 295 and 523 K. The HIP interfaces possessed many precipitates, and enriched peak spectrum of chromium was detected from the precipitates. In addition, aspect of the spectrum was qualitatively equivalent to that of MC in grain boundaries of F82H steel. In result, the HIP boundary has many MC which were generally seen in grain boundaries of F82H steel. Rupture did not occur in the HIP interface. In result, it can be mentioned that bondability is maintained under the irradiation and testing conditions. The strength and elongation of the HIP-bonded region decreased somewhat in comparison with the results of an IEA standard steel.

Neutronics assessment of advanced shield materials using metal hydride and borohydride for fusion reactors

Hayashi, Takao; Tobita, Kenji; Nishio, Satoshi; Ikeda, Kazuki*; Nakamori, Yuko*; Orimo, Shinichi*; DEMO Plant Design Team

Fusion Engineering and Design, 81(8-14), p.1285 - 1290, 2006/02

https://doi.org/10.1016/j.fusengdes.2005.09.060

Neutron transport calculations were carried out to evaluate the capability of metal hydrides and borohydrides as an advanced shielding material. Some hydrides indicated considerably higher hydrogen content than polyethylene and solid hydrogen. The hydrogen-rich hydrides show superior neutron shielding capability to the conventional materials. From the temperature dependence of dissociation pressure, ZrH and TiH can be used without releasing hydrogen at the temperature of less than 640 C at 1 atm. ZrH and Mg(BH) can reduce the thickness of the shield by 30% and 20% compared to a combination of steel and water, respectively. Mixing some hydrides with F82H produces considerable effects in -ray shielding. The neutron and -ray shielding capabilities decrease in order of ZrH Mg(BH) and F82H TiH and F82H water and F82H.

Key achievements in elementary R&D on water-cooled solid breeder blanket for ITER test blanket module in JAERI

Suzuki, Satoshi; Enoeda, Mikio; Hatano, Toshihisa; Hirose, Takanori; Hayashi, Kimio; Tanigawa, Hisashi; Ochiai, Kentaro; Nishitani, Takeo; Tobita, Kenji; Akiba, Masato

Nuclear Fusion, 46(2), p.285 - 290, 2006/02

https://doi.org/10.1088/0029-5515/46/2/012

This paper presents significant progress in R&D of key technologies on the water-cooled solid breeder blanket for the ITER-TBM in JAERI. By the improvement of heat treatment process for blanket module fabrication, a fine-grained microstructure of F82H, can be obtained by homogenizing it at 1150 C followed by normalizing at 930 C after the HIP process. Moreover, a promising bonding process for a tungsten armor and an F82H structural material was developed by using a uniaxial hot compression without any artificial compliant layer. Also, it has been confirmed that a fatigue lifetime correlation, which was developed for ITER divertor, can be applicable for F82H first wall mock-up. As for R&D on a breeder material, LiTiO, the effect of compression loads on thermal conductivity of pebble beds has been clarified. JAERI have extensively developed key technologies for ITER-TBM, and now steps up into an engineering R&D stage, where integrated performance of TBM structures will be demonstrated by scalable mock-ups.

Radiation hardening and -embrittlement due to He production in F82H steel irradiated at 250 C in JMTR

Wakai, Eiichi; Jitsukawa, Shiro; Tomita, Hideki*; Furuya, Kazuyuki; Sato, Michitaka*; Oka, Keiichiro*; Tanaka, Teruyuki*; Takada, Fumiki; Yamamoto, Toshio*; Kato, Yoshiaki; et al.

Journal of Nuclear Materials, 343(1-3), p.285 - 296, 2005/08

https://doi.org/10.1016/j.jnucmat.2004.10.167

The dependence of helium production on radiation-hardening and -embrittlement has been examined in a reduced-activation martensitic F82H steel doped with B, B and B+B irradiated at 250C to 2.2 dpa. The total amounts of doping boron were about 60 massppm. The range of He concentration produced in the specimens was from about 5 to about 300 appm. Tensile and fracture toughness tests were performed after neutron irradiation. 50 MeV-He irradiation was also performed to implant about 85 appm He atoms at 120C by AVF cyclotron to 0.03 dpa, and small punch testing was performed to obtain DBTT. Radiation-hardening of the neutron-irradiated specimens increased slightly with increasing He production. The 100 MPam DBTT for the F82H+B, F82H+B+B, and F82H+B were 40, 110, and 155C, respectively. The shifts of DBTT due to He production were evaluated as about 70C by 150 appmHe and 115C by 300 appmHe. The DBTT shift in the small punch testing was evaluated as 50C.

Hydrogen permeation measurement of the reduced activation ferritic steel F82H by the vacuum thermo-balance method

Yoshida, Hajime; Kosaku, Yasuo*; Enoeda, Mikio; Abe, Tetsuya; Akiba, Masato

JAERI-Research 2005-003, 13 Pages, 2005/03

JAERI-Research-2005-003.pdf:3.33MB

Hydrogen permeation fluxes of the reduced activation ferritic steel F82H were quantitatively measured by a newly proposed method, vacuum thermo-balance method, for a precise estimation of tritium leakage in a fusion reactor. We prepared sample capsules made of F82H, which enclosed hydrogen gas. The hydrogen in the capsules permeated through the capsule wall, and subsequently desorbed from the capsule surface during isothermal heating. The vacuum thermo-balance method allows simultaneous measurement of the hydrogen permeation flux by two independent methods, namely, the net weight reduction of the sample capsule and exhaust gas analysis. Thus the simultaneous measurements by two independent methods increase the reliability of the permeability measurement. The ratio of the hydrogen permeation fluxes obtained by the net weight reduction to that measured by the exhaust gas analysis was in the range from 1/4 to 1/1 in this experiment. It has been demonstrated that the vacuum thermo-balance method is effective for the measurement of hydrogen permeation rate of F82H.

Post irradiation plastic properties of F82H derived from the instrumented tensile tests

Taguchi, Tomitsugu; Jitsukawa, Shiro; Sato, Michitaka*; Matsukawa, Shingo*; Wakai, Eiichi; Shiba, Kiyoyuki

Journal of Nuclear Materials, 335(3), p.457 - 461, 2004/12

https://doi.org/10.1016/j.jnucmat.2004.08.001

F82H (Fe-8Cr-2W) and its variant doped with 2%Ni were irradiated up to 20 dpa at 300C in the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory. Post irradiation tensile testing was performed at room temperature. During testing, the images of the specimens including the necked region were continuously recorded. Tests on cold worked material were also carried out for comparison. From the load-displacement curves and the strain distributions obtained from the images, flow stress levels and strain hardening behavior was evaluated. A preliminary constitutive equation for the plastic deformation of irradiated F82H is presented. The results suggest that the irradiation mainly causes defect-induced hardening while it did not strongly affect strain hardening at the same flow stress level for F82H irradiated at 300C. The strain hardening of Ni doped specimens was, however, strongly affected by irradiation. Results provide basics to determine allowable stress levels at temperatures below 400C.

Fabrication of model for fusion nuclear first wall made from F82H steel by HIP method and the metallurgical and mechanical properties

Furuya, Kazuyuki

JAERI-Research 2004-013, 165 Pages, 2004/09

JAERI-Research-2004-013.pdf:53.73MB

no abstracts in English

Microstructure property analysis of HFIR-irradiated reduced-activation ferritic/martensitic steels

Tanigawa, Hiroyasu; Hashimoto, Naoyuki*; Sakasegawa, Hideo*; Klueh, R. L.*; Sokolov, M. A.*; Shiba, Kiyoyuki; Jitsukawa, Shiro; Koyama, Akira*

Journal of Nuclear Materials, 329-333(1), p.283 - 288, 2004/08

https://doi.org/10.1016/j.jnucmat.2004.04.053

Reduced-activation ferritic/martensitic steels (RAFs) were developed as candidate structural materials for fusion power plants. In a previous study, it was reported that ORNL9Cr-2WVTa and JLF-1 (Fe-9Cr-2W-V-Ta-N) steels showed smaller ductile-brittle transition temperature (DBTT) shifts compared to IEA modified F82H (Fe-8Cr-2W-V-Ta) after neutron irradiation up to 5 dpa at 573K. This difference in DBTT shift could not be interpreted as an effect of irradiation hardening, and it is also hard to be convinced that this difference was simply due to a Cr concentration difference. To clarify the mechanisms of the difference in Charpy impact property between these steels, various microstructure analyses were performed.

Analysis of Ta-rich MX precipitates in RAFs

Tanigawa, Hiroyasu; Sakasegawa, Hideo*; Hashimoto, Naoyuki*; Zinkle, S. J.*; Klueh, R. L.*; Koyama, Akira*

Fusion Materials Semiannual Progress Report for the Period Ending (DOE/ER-0313/35), p.33 - 36, 2004/04

Extraction replica samples were prepared from F82H-IEA, F82H HT2, JLF-1 and ORNL9Cr to analyze the precipitate distribution. The samples were examined to obtain precipitate size distribution with TEM and to analyze chemical composition distribution with SEM. Back-scattered electron imaging was found to be the effective way to separate Ta-rich precipitate from other precipitates. Results showed that most of the precipitates were M23C6, and the shape is a round ellipsoid in F82H-IEA and HT2, but was a long ellipsoid in JFL-1 and ORNL9Cr. It was also found that MX precipitates were few and large and contain Ti in F82H-IEA and HT2, but a lot of fine MX precipitates without Ti were observed in JLF-1 and ORNL9Cr.